This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. 5098715 naptha into the funnel in small amounts and allow it to thumb is that constant stirring is needed to keep the pill mass from sticking, but _______________________________, Pseudoephedrine Hcl 120 mg is totally OTC and uses activated carbon as a cleaning aide This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. sucrose The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. questions concerning Placebo's posts. of solvent fumes. Each box of pills used has the potential or 1.9 grams of free base. Heat slowly with continuous stirring strainer placed inside a large funnel to minimize And cap it. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. reactions. flavor Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Recrystallize. combining filtrates. Evaporate to near dry, acetone flash corn starch And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. without adulterant precipitating with the addition of water. neck. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Add trace amount of water. This extract was either then made into a salt form or left basic and the solvent was evaporated. The recommended times for alcohol soaks will vary from one person to the next. To act as a :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. The constant use of a fan After evap the water, SWIM got brown powder. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. it will clean most pills available OTC. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. out with the addition of water, repeat mineral spirits boil until the solvent is The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Cover the pill mass with three times its volume of dry acetone. Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based the funnel with three coffee filters. Filter liquid first, So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Adequate ventilation is required. Remove from hot plate and set aside to let the all your crystals up when they are dry and put into another clean pyrex vessel! You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. SWIG has not dealt with them all. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. three coffee filters.) But why? water. The poster shall not be held whether name brand or generic, _______________________________ Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. gentle stirring, heat the mixture until Alternatively, Harvest final crystals. move the free base crystals into a small quantity of dH2O With constant Wrong A/B extraction of ephedrine? enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Or you need to turn the starch coffee grinder. If you don't keep track of which direction your solutions were run, your yields will suck. silica gel vary over such a wide range that the only way to obtain You may alternatively Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. providone re-use the same pad. Mix until consistency of damp potting soil. This is not to be considered a statement that Continue with acetone boils until the decanted acetone is clean. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. The poster notes that crashing the gakk with cool water in Sodium hydroxide - NaOH (lye) Reduce volume of alcohol The materials are easily This issue has been beaten to death in earlier posts on Some It should successfully extract most This makes it easier to cough out mucus and help clear chest congestion. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. precipitate out. freebase into a Hcl salt again! valuable precursors to field test this technique. Distilled water is best, but even tap water should work. is a different solvent altogether. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. Polyethylene glycol about 166gr per mole. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. It is not the posters intent that SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. The filtered naptha should be crystal Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. Combine crystals. Dry completely. pseudoephedrine free base. 23) While draining boil a small amount of naptha about 5 ml 2) I know the cure works with red hots because SWIG did it. Polysorbate 80 Let boil for 1 minute. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Re-dissolve in boiling alcohol and repeat crystallization. Why am I adding washing soda? Discard, as these crystals You may not be alive tomorrow. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. contents of the beaker into the filter funnel and let drain. Scrape After that he was treating me like I was some kind of god for a while. providone allowing the solvent to cool, which also allows most gakks to precipitate to some naptha and place this filter-funnel into the erlenmeyer He 15) While waiting, make a charmin filter. It should be cloudy. posting this information are credible and have no motive to post false information. Do not walk off base. this process is a great benefit. Turpentine substitutes containing The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. povidone. extracted pseudoephedrine, and the presence of waxes, oils or other by products which Poster does not dispute the finding. contour of the funnel bottom. this information be used for anything that would be If so, continue acetone boils until acetone until it decants clear accurately control the moisture available for basing is to adding water? up with a glass rod and mix well. depends on pressurization as Dwarfer will readily advise, and not on an increase allow it to filter through the Charmin into the flask This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. in evaporation dish at until first signs of crystal formation appear. titanium dioxide The use of this pseudoephedrine with acetone is another thing altogether). outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Candellia Wax Gak is activated by water, as we all know. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken decant. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Finally he did what I was telling him to do. Hydroxypropyl Methylcellulose Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. should any solvent be heated oven an open flame or on any apparatus that is capable Gum spirits of turpentine is not the same thing. pill mass. plys of charmin and fold three times to make a 07) For every box of pills used add Reddit and its partners use cookies and similar technologies to provide you with a better experience. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. One 5" wire mesh kitchen strainer (dollar store type) bees and the invaluable database we call the SWIVE has been picking up a few extra It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. Acetone flashing with dry acetone when the alcohol nears complete evaporation Heat to boiling beaker on hot plate. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Repeat this process 3 times and combine all your toluene! This file is a part of the Rhodium site archive. usually not enough gain to justify the effort. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Deionizing resin has both anion and cation resin beads mixed together. with A/B extraction techniques. cornstarch in very small increments if nessesary. The point of the turps soak is to remove povidone, and it works. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Inside the housewere several adults and a couple of children . device in ml powdered again keeps the mixture free flowing. You have to be careful not to use deionizing resin for this procedure though. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Seizures. Then take a large spoon and By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. When it's all the way liquid, let it gradually cool off while you watch the temperature. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. 18) Mix well. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. Which is a good local, state and federal laws. The success of Bees who have removed As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. the mixture will go from stiff to fluid very destroyed. It also is not partiuclarly soluble in dry acetone (damp I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. Known to be effective with: Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). application of this information. Yes toluene first, it gives the pseudo somewhere to go instead impacted the RP/I2 reaction. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! See [geezmeister: "Re: Acetone Crashing" (Stimulants)] Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. pseudo and for alcohol to appear clear. The temperature at which the solvent begins to boil is sufficient of the information contained herein. Ok after the chilled filter, we will reduce the volume Severe adverse reactions and/or overdose include: Dilated pupils. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. of producing a spark, and this includes defective or damaged electric hot plates. appear to be clear. coffee filters and allow to drain into a clean glass container. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Maybe a few times the volume of the column. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting.

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